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#DIARLY KETONE SYNTHESIS HOW TO#
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Permission is not required) please go to the Copyright If you want to reproduce the wholeĪrticle in a third-party commercial publication (excluding your thesis/dissertation for which If you are the author of this article, you do not need to request permission to reproduce figuresĪnd diagrams provided correct acknowledgement is given. Provided correct acknowledgement is given. If you are an author contributing to an RSC publication, you do not need to request permission NMR spectra of all the diaryl acrylates (except 2a and 2m) indicated the presence of E and Z isomers in solution (CDCl3). Please go to the Copyright Clearance Center request page. Under this improved condition, other diaryl ketones also reacted with ethyl cyanoacetate to yield the corresponding diaryl acrylates 2bd and 2hi in moderate to good yields. To request permission to reproduce material from this article in a commercial publication, Provided that the correct acknowledgement is given and it is not used for commercial purposes. This article in other publications, without requesting further permission from the RSC, Wang,Ĭreative Commons Attribution-NonCommercial 3.0 Unported Licence. Continuous flow synthesis of diaryl ketones by coupling of aryl Grignard reagents with acyl chlorides under mild conditions in the ecofriendly solvent 2-methyltetrahydrofuranĬ.